📋 Case Study

FCC Regenerator Thermal Runaway Mitigation

Unstable regenerator temperature excursions (>730°C) causing catalyst sintering and CO spikes

🏗️ Project Overview

Refinery in Texas upgrading fluid catalytic cracking unit after catalyst change

🎯 Challenge

Unstable regenerator temperature excursions (>730°C) causing catalyst sintering and CO spikes

🔧 Design Approach

Dynamic kinetic model coupling coke combustion rate, heat release, and flue gas residence time; installed distributed thermocouples and O₂ trim control

📐 Design Diagram

RegeneratorTCTCTCFlue GasO₂ Trim+/-r_coke = 0.82 g/g·minT > 730°C → sintering/CO↑T_ad = 825°Cτ_CO = 12.7 sFCC Regenerator Thermal Runaway Mitigation

AI-generated project design illustration

📐 Key Calculations

Coke Combustion Rate

r_coke = k * X_coke * P_O2^n
Result: 0.82 g coke/g cat·min
Validated via TGA and microreactor data

Adiabatic Flame Temperature (T_ad)

T_ad = T_in + (−ΔH_coke * X_coke) / (Σ Cp_i * y_i)
Result: 825°C
Explained observed peak temperatures

CO Oxidation Delay Time

τ_CO = 1/k_CO * ln(CO_in/CO_out)
Result: 12.7 s
Confirmed insufficient residence time for complete CO burnout

📊 Results

Regenerator outlet temp stabilized at 705±3°C, CO emissions reduced by 92%, catalyst life extended by 35%

💡 Lessons Learned

  • Coke oxidation kinetics are strongly inhibited by steam—ignored in legacy models
  • Thermocouple placement depth affects measured lag and false-positive runaway alarms
  • Dynamic model must include catalyst inventory heat capacity as state variable

Key Takeaways

  • 1Coke oxidation kinetics are strongly inhibited by steam—ignored in legacy models
  • 2Thermocouple placement depth affects measured lag and false-positive runaway alarms
  • 3Dynamic model must include catalyst inventory heat capacity as state variable